Analytical Chemistry Experiment (Vol. 5)
Author: Wuhan University Editor Published: 2011
Series items: Brief introduction to the contents of the 11th Five-Year National Plan for General Higher Education. Analytical Chemistry Experiment (Fifth Edition, Volume 1) edited by Wuhan University is based on Analytical Chemistry Experiment (Fourth Edition). Into. The book includes eleven chapters: basic knowledge of analytical chemistry experiments, qualitative analysis experiments of common ions, quantitative analysis instruments and operating methods, basic operation experiments of quantitative analysis, acid-base titration experiments, complex titration experiments, redox titration experiments, precipitation titration And gravimetric experiments, spectrophotometric experiments, common separation and enrichment method experiments, and comprehensive experiments. Compared with the previous version, some new experiments have been added, and some outdated content has also been deleted. Analytical Chemistry Experiment (Fifth Edition, Vol. 1) is comprehensive, diverse, and closely related to reality. It can be used as a comprehensive university chemistry, applied chemistry, materials chemistry, environmental science, geology and other professional analytical chemistry experimental teaching materials, and can also be used as a reference for higher professional colleges and engineering colleges.
Chapter 1 Basics of Analytical Chemistry Experiments § 1.1 Requirements for Analytical Chemistry Experiments § 1.2 Laboratory Safety Knowledge § 1.3 Overview of Quantitative Analysis Experiments Chapter 2 Qualitative Analysis Experiments for Common Ions § 2.1 Introduction to Qualitative Analysis § 2.2 Semi-Quantitative Qualitative Analysis Commonly used instruments and basic operations §2.3 Qualitative analysis experiment experiment one cation group I experiment two cation group IIA experiment three cation group IIB experiment four cation group III experiment five cation group IV experiment six cation group V experiment seven cation Ⅰ Analytical experiments of ～～ groups of ions Eight Analytical experiments of common anions Qualitative analysis of nine copper alloys §2.4 Qualitative analysis reagent preparation method Chapter 3 Quantitative analysis instruments and operating methods §3.1 Titration analysis instruments and operating methods §3.2 Precipitation gravimetric analysis Operation and Instrument §3.3 Analytical Balance §3.4 Acidity Meter §3.5 Spectrophotometer Chapter 4 Quantitative Analysis Basic Operation Experiment Experiment 1 Analytical Balance Weighing Exercise Experiment 2 Titration Analysis Operation Exercise Experiment 3 Capacity Instrument Calibration Chapter 5 Acid-Base Titration Experiment Experiment 1 Determination of the molar mass of organic acids (constant, micro titration) Experiment 2 Determination of total acidity of edible vinegar (constant, micro titration) Experiment 3 Determination of acetylsalicylic acid content in aspirin tablets Experiment 4 Determination of sodium acetate content by non-aqueous titration experiment Experiment 5 Potential titration experiment of HCI-HAC mixed solution Preparation and buffer solution Determination of pH VII Determination of dissociation degree and dissociation constant of acetic acid Design experiments of octanoic acid-base titration Chapter 6 Complexation titration experiment Experiment 1 Calibration of EDTA solution Experiment 2 Determination of tap water hardness Experiment 3 Continuous titration of Bi3 + Pb2 mixed solution Experiment 4 Determination of aluminum content in aluminum alloy Experiment determination of A1 (OH) 2 and MGO content in Wuweishuping tablets Experiment 6 complex titration design experiment Chapter 7 Redox titration experiment Experiment 1 Determination of hydrogen peroxide content Experiment 2 Chemical requirements Determination of oxygen content. Three. Determination of total iron content in iron ore. Experiment four. Iodine determination method for determination of copper content in copper alloys. Experiment five. Vitamin C preparation and direct determination of ascorbic acid content in fruits and vegetables. Experiment six. Calcium content in calcium supplements. Determination of Phenol by Heptabromide Method Experiment of Oxidation-Reduction Titration Design Experiment Chapter 8 Precipitation Titration and Gravimetric Analysis Experiment 1 Moore method to determine the content of chlorine in soluble chloride Experiment 2 Verhard method to determine the content of chlorine in soluble chloride Experiment 3 Determination of the content of soluble barium salt Experiment 4 Microwave drying constant weight method to determine the content of soluble barium salt Barium content experiment. Five. Determination of nickel content in iron and steel. Six. Determination of potassium content in plants or fertilizers. Seven. Precipitation titration design experiment. Chapter 9. Spectrophotometric experimental experiment. Conditional test and determination of iron by o-phenanthroline spectrophotometry. Determining the composition of the composition. Determination of trace iron by vicinal phenanthroline spectrophotometry. Determination of trace copper by catalytic kinetic spectrophotometry with trializarin red S. Determination of phosphorus content in raw (cast) iron and steel by tetraphosphor molybdenum blue spectrophotometry. Chapter 10 Common Separation and Enrichment Methods Experiment Experiment 1 Extraction Separation-Spectrophotometric Determination of Trace Lead in Environmental Water Samples Experiment Ion Exchange Separation of Cobalt and Nickel and Determination of Complex Titration Experiment 3 Extraction and Thin Layer of Natural Pigments in Vegetables Chromatographic Separation Experiment Four Microwave-Assisted Extraction-Spectrophotometric Determination of Total Flavonoids in Bamboo Leaves Chapter 11 Comprehensive Experimental Experiments SiO2 and Fe2O in Portland Cement 3, A12O3, CaO and MgO content determination experiment II Determination of formaldehyde content in indoor air Experiment preparation and composition analysis experiment of trichloride pentachloramine (Ⅲ) tetrazinc passivation solution analysis experiment five electrolytic refined salt Water analysis experiment 6 Water quality analysis experiment of open-air water body 7 Determination of copper and zinc content in appendix Appendix 1 Common indicator Appendix 2 Preparation of common buffer solution Appendix 3 Density and concentration of commonly used concentrated acids and bases Appendix 4 Common reference materials And its drying conditions and applications Appendix 5 Common fluxes and crucibles Appendix 6 Relative atomic mass table (2001) Appendix 7 Relative molecular mass tables of commonly used compounds Appendix 8 List of commonly used instruments for quantitative chemical analysis experiments Appendix 9 Common tolerances for constant volume glass instruments Appendix 10 Models and properties of domestic filter papers Appendix 11 Titration analysis test operation checklist (take the calibration of NAOH solution concentration as an example) Appendix 12 Main reference of commonly used analytical chemistry terms (Chinese-English)